烧结压力对铜粉放电等离子烧结的影响规律

Influence of Sintering Pressure on the SPS of Powdered Copper

  • 摘要: 研究了平均粉末粒度为1μm的铜粉在不同压力条件下的放电等离子烧结过程,系统分析了压坯的密度和微观组织与烧结升温阶段的初始压力和保压压力之间的关系.结果表明:烧结温度为800℃,初始压力为1 MPa,保压压力为50 MPa的烧结工艺,可以制备相对密度大于98%,平均晶粒度小于10μm的烧结铜.同时发现,采用SPS工艺制备的烧结铜沿厚度方向存在不同于传统双向压制的密度分布,SPS烧结铜的表面密度低于心部密度.

     

    Abstract: Powdered copper having an average powder size of 1?μm was sintered by spark plasma sintering(SPS) at different sintering pressure.The relationship of relative density and microstructure of compact to initial pressure during the heating up period and dwelling pressure is studied.Results showed that the relative density of sintered copper was above 98% and its grain fineness was about 10?μm,when sintered by the process of loading 1?MPa as initial pressure and 50?MPa as the dwelling pressure,and a sintering temperature at 800?℃.In the mean time,the density distribution of sintered copper made by SPS along depth was different to the compact made by traditional double-action compacting.Its surface density is lower than the central density.

     

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